反应条件
1.1: n-BuLi / diethyl ether; hexane / 1 h / -10 °C
1.2: 76 percent / diethyl ether; hexane; tetrahydrofuran / 2 h / -10 - 80 °C
2.1: 86 percent / quinoline; H2 / Pd-CaCO3 / methanol / 8 h / 20 °C
3.1: 22 percent / triethylamine; tributyltin hydride / palladium(II) acetate / CH2Cl2 / 18 h / Heating
View Scheme
参考文献
In, Su Kim; Guang, Ri Dong; Young, Hoon Jung
Journal of Organic Chemistry, 2007 , vol. 72, # 14 p. 5424 - 5426