bromine in dichloromethane
T=-55°C; 1.5 h; in the dark;
参考文献
Ellis-Davies, Graham C. R.; Gilbert, Andrew; Heath, Peter; Lane, Jon C.; Warrington, John V.; Westover, David L.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , p. 1833 - 1842
1: bromine / CH2Cl2 / 1.5 h / -55 °C / in the dark
2: aluminum chloride / CH2Cl2 / 1.25 h
3: 18.5 g / sodium hypobromite / dioxane
4: thionyl chloride / benzene / 2 h / Heating
5: aqueous ammonia
6: thionyl chloride / benzene / 6 h / Heating
7: acetic acid, zinc powder / ethanol / 1.25 h / Heating
View Scheme
参考文献
Ellis-Davies, Graham C. R.; Gilbert, Andrew; Heath, Peter; Lane, Jon C.; Warrington, John V.; Westover, David L.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , p. 1833 - 1842
