2-甲基-6-苯基苯并噻唑合成路线 (共 7 条)
反应条件
potassium phosphate; C58H72N2O4P2Pd2 in tert-butyl alcohol T=110°C; Suzuki-Miyaura cross-coupling; 3 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 42 p. 8059 - 8063
反应条件
CM-phos; tetrabutyl ammonium fluoride; palladium diacetate; acetic acid in tert-butyl alcohol T=90°C; Hiyama cross-coupling; 16 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 11, # 2 p. 317 - 320
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran T=20°C; 0.5 h;
参考文献
Russian Chemical Bulletin, , vol. 42, # 11 p. 1925 - 1926
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2008 - 2009
反应条件
air; potassium carbonate; palladium dichloride in water T=100°C; 2 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 32, # 12 p. 1803 - 1811
反应条件
phenyl-magnesium bromide in tetrahydrofuran Ambient temperature13-18 h; Yields of byproduct given;
参考文献
Russian Journal of Organic Chemistry, , vol. 32, # 12 p. 1803 - 1811
反应条件
in tetrahydrofuran Ambient temperature13-18 h; Yield given;
参考文献
Russian Journal of Organic Chemistry, , vol. 32, # 12 p. 1803 - 1811