6-氨基-5-甲氧基吲哚-2-甲酸乙酯合成路线 （共 3 条）
反应条件
hydrogenchloride in acetone T=80°C; 4 h;
参考文献
Martin, Pierre; Steiner, Eginhard; Auer, Kurt; Winkler, Tammo
Helvetica Chimica Acta, 1993 , vol. 76, # 4 p. 1667 - 1673
反应条件
1: 73 percent / CH2Cl2 / 8 h / Ambient temperature 2: 94.5 percent / Cu(OAc)2*H2O, HCl(g)/air / CH2Cl2 3: 69 percent / Ce(NH4)2(NO3)6 / acetonitrile; H2O / 0.5 h / -3 °C 4: 63 percent / LiOH*H2O / tetrahydrofuran; H2O / 20.5 h / Ambient temperature; purification with conc. H2SO4 View Scheme
参考文献
Helvetica Chimica Acta, , vol. 76, # 4 p. 1667 - 1673
反应条件
1: 73 percent / CH2Cl2 / 8 h / Ambient temperature
2: 94.5 percent / Cu(OAc)2*H2O, HCl(g)/air / CH2Cl2
3: 69 percent / Ce(NH4)2(NO3)6 / acetonitrile; H2O / 0.5 h / -3 °C
View Scheme
参考文献
Martin, Pierre; Steiner, Eginhard; Auer, Kurt; Winkler, Tammo
Helvetica Chimica Acta, 1993 , vol. 76, # 4 p. 1667 - 1673
