6,7-二甲基-1,2,3,4-四氢萘合成路线 (共 9 条)
反应条件
hydrogen; palladium on activated charcoal in cyclohexane T=110°C; P=30002.4 Torr; 2 h; Title compound not separated from byproducts;
参考文献
Laurens, T.; Schmit-Quiles, F.; Nicole, D.
Magnetic Resonance in Chemistry, 1995 , vol. 33, # 7 p. 523 - 528
反应条件
ethanol; nickel T=110°C; P=51485.6 Torr; Hydrogenation;
参考文献
Coulson
Journal of the Chemical Society, 1938 , p. 1305,1310
反应条件
tetra-n-propyl-diborane; hydrogen in n-heptane T=200°C; P=75006 Torr; 4 h;
参考文献
Yalpani, Mohamed; Lunow, Thomas; Koester, Roland
Chemische Berichte, 1989 , vol. 122, p. 687 - 694
反应条件
ammonia; lithium T=-78°C; 0.75 h;
参考文献
Atwal, Karnail S.; O'Reilly, Brian C.; Ruby, Eric P.; Turk, Chester F.; Aberg, Gunnar; et al.
Journal of Medicinal Chemistry, 1987 , vol. 30, # 4 p. 627 - 635
反应条件
1: hydroquinone / 110 °C 2: P2O5 / 175 - 225 °C View Scheme
参考文献
Skwartschenko et al.
Vestnik Moskovskogo Universiteta, 1958 , vol. 13, # 5 p. 187,189
Chem.Abstr., 1959 , p. 12249
反应条件
1: hydroquinone / 110 °C 2: P2O5 / 175 - 225 °C View Scheme
参考文献
Skwartschenko et al.
Vestnik Moskovskogo Universiteta, 1958 , vol. 13, # 5 p. 187,189
Chem.Abstr., 1959 , p. 12249
反应条件
aluminium trichloride
参考文献
Lagidze,B.M.; Loladze,N.R.
J. Gen. Chem. USSR (Engl. Transl.), 1962 , vol. 32, # 5 p. 1627 - 1633,1610 - 1615
反应条件
Pd-BaSO4 T=290 - 300°C;
参考文献
Kloetzel; Herzog
Journal of the American Chemical Society, 1950 , vol. 72, p. 1991,1993
参考文献
Journal of the American Chemical Society, , vol. 70, p. 2791