2-(4-甲氧基苯基)-2-氧代乙醛合成路线 （共 34 条）
反应条件
dimethyl sulfoxide in water T=50°C; 2.5 h;
参考文献
MITSUBISHI PHARMA CORPORATION; SANOFI-SYNTHELABO
Patent: WO2004/85408 A1, 2004 ;
Location in patent: Page 262 ;
WO 2004/085408 A1
反应条件
selenium (IV) oxide in 1,4-dioxane; water Heating;
参考文献
Reid, Caroline M.; Ebikeme, Charles; Barrett, Michael P.; Patzewitz, Eva-Maria; Mueller, Sylke; Robins, David J.; Sutherland, Andrew
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 7 p. 2455 - 2458
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide T=20°C; 0.5 h; Inert atmosphere;
参考文献
Yang, Yan; Gao, Meng; Deng, Cong; Zhang, Dong-Xue; Wu, Liu-Ming; Shu, Wen-Ming; Wu, An-Xin
Tetrahedron, 2012 , vol. 68, # 31 p. 6257 - 6262
反应条件
dimethyl sulfoxide; copper(II) oxide T=65°C; 2.5 h;
参考文献
Yin, Guodong; Zhou, Baohan; Meng, Xianggao; Wu, Anxin; Pan, Yuanjiang
Organic Letters, 2006 , vol. 8, # 11 p. 2245 - 2248
反应条件
sodium acetate in dimethyl sulfoxide T=20°C; 16 h;
参考文献
Lahue, Brian R.; Lo, Sie-Mun; Wan, Zhao-Kui; Woo, Grace H. C.; Snyder, John K.
Journal of Organic Chemistry, 2004 , vol. 69, # 21 p. 7171 - 7182
反应条件
2-Hydroxypyridine T=20°C;
参考文献
Katritzky, A. R.; Chapman, A. V.; Dowlatshahi, H. M.
Acta Chimica Academiae Scientiarum Hungaricae, 1981 , vol. 107, p. 315 - 320
反应条件
1: isopropylmagnesium chloride / tetrahydrofuran / -78 - 0 °C / Inert atmosphere 2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 19 h / 20 °C 3: dimethyl sulfoxide / 40 h / 60 °C View Scheme
参考文献
Zall, Andrea; Bensinger, Dennis; Schmidt, Boris
European Journal of Organic Chemistry, 2012 , # 7 p. 1439 - 1447
反应条件
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 19 h / 20 °C 2: dimethyl sulfoxide / 40 h / 60 °C View Scheme
参考文献
Zall, Andrea; Bensinger, Dennis; Schmidt, Boris
European Journal of Organic Chemistry, 2012 , # 7 p. 1439 - 1447
反应条件
chloroform; ozone und folgende Zersetzung mit Wasser;
参考文献
Weygand
Justus Liebigs Annalen der Chemie, 1927 , vol. 459, p. 112
Justus Liebigs Annalen der Chemie, 1929 , vol. 472, p. 178
参考文献
Fodor; Kovacs
Journal of the American Chemical Society, 1949 , vol. 71, p. 1045,1047
