N-丁基-1-苯基甲亚胺合成路线 （共 25 条）
反应条件
1: acetic acid / methanol / 2.5 h / 20 °C / Inert atmosphere 2: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran; isopropyl alcohol / 0 - 20 °C / Inert atmosphere 3: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere View Scheme
参考文献
Greger, Jessica G.; Yoon-Miller, Sarah J. P.; Bechtold, Nathan R.; Flewelling, Scott A.; MacDonald, Jacob P.; Downey, Catherine R.; Cohen, Eric A.; Pelkey, Erin T.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8203 - 8214
反应条件
acetic acid 4 h; Heating;
参考文献
Singh, Harjit; Sarin, Rakesh
Journal of Chemical Research, Miniprint, 1988 , # 10 p. 2623 - 2640
反应条件
ruthenium trichloride; triphenylphosphine in 1,4-dioxane T=180°C; 40 h;
参考文献
Angewandte Chemie, International Edition, , vol. 40, # 5 p. 958 - 960
Angewandte Chemie, , vol. 113, p. 984 - 986
反应条件
methyltrioxorhenium (VII)
参考文献
Zhu, Zuolin; Espenson, James H.
Journal of Organic Chemistry, 1995 , vol. 60, # 22 p. 7090 - 7091
参考文献
Wegler et al.
Angewandte Chemie, 1958 , vol. 70, p. 351,365
反应条件
ruthenium trichloride; triphenylphosphine in 1,4-dioxane T=180°C; 40 h;
参考文献
Angewandte Chemie, International Edition, , vol. 40, # 5 p. 958 - 960
Angewandte Chemie, , vol. 113, p. 984 - 986
反应条件
in chloroform-d1 T=25°C; Equilibrium constantKinetics;
参考文献
Ciaccia, Maria; Pilati, Silvia; Cacciapaglia, Roberta; Mandolini, Luigi; Di Stefano, Stefano
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 20 p. 3282 - 3287
反应条件
in acetonitrile-D3 T=25°C; Kinetics; Solvent;
参考文献
Ciaccia, Maria; Cacciapaglia, Roberta; Mencarelli, Paolo; Mandolini, Luigi; Di Stefano, Stefano
Chemical Science, 2013 , vol. 4, # 5 p. 2253 - 2261
反应条件
sodium tetrahydroborate in methanol T=5°C;
参考文献
Garrido, Daniel O. Alonso; Buldain, Graciela; Frydman, Benjamin
Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 2021 - 2023
反应条件
in benzene-d6 T=50°C; 37 h; Inert atmosphereSealed tube;
参考文献
Frazier, Brenda A.; Williams, Valerie A.; Wolczanski, Peter T.; Bart, Suzanne C.; Meyer, Karsten; Cundari, Thomas R.; Lobkovsky, Emil B.
Inorganic Chemistry, 2013 , vol. 52, # 6 p. 3295 - 3312
