6-甲氧基-1-萘满酮合成路线 (共 219 条)
反应条件
1: 1.) BuLi / 1.) hexane, THF, -10 deg C, 2 h, 2.) -10 deg C, 2.5 h 2: silver triflate / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Australian Journal of Chemistry, , vol. 43, # 5 p. 815 - 824
反应条件
1: KOH / methanol 2: (methylation) View Scheme
参考文献
Tetrahedron, , vol. 18, p. 1355 - 1367
反应条件
1: CrO3, aq. AcOH, Ac2O 2: KOH / methanol 3: (methylation) View Scheme
参考文献
Tetrahedron, , vol. 18, p. 1355 - 1367
反应条件
oxygen; Titanium(IV) oxide in acetonitrile Bi(OAc)3 filter;
参考文献
Tetrahedron, , vol. 41, # 19 p. 4107 - 4118
反应条件
silver trifluoromethanesulfonate in dichloromethane 2 h; Ambient temperature; Yield given;
参考文献
Australian Journal of Chemistry, , vol. 43, # 5 p. 815 - 824
反应条件
silver trifluoromethanesulfonate in dichloromethane 2 h; Ambient temperature; Yield given;
参考文献
Australian Journal of Chemistry, , vol. 43, # 5 p. 815 - 824
反应条件
silver trifluoromethanesulfonate in dichloromethane 2 h; Ambient temperature; Yield given;
参考文献
Australian Journal of Chemistry, , vol. 43, # 5 p. 815 - 824
反应条件
1.1: 930 mg / NaHCO3 / CH2Cl2 / 2.5 h 2.1: iodobenzene bistrifluoroacetate / CH2Cl2 / 20 °C 2.2: 6 percent / BF3*Et2O / CH2Cl2 View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 4 p. 513 - 528
反应条件
1: 6 N aq. KOH / ethanol / 2 h / Heating 2: polyphosphoric ester / CHCl3 / 7 h / Ambient temperature View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 29, # 4 p. 477 - 480
反应条件
1: 93 percent / NaBH4 2: H2O, MgCO3 / dioxane / 22 h / Heating 3: 67 percent / NaOH / tetrahydrofuran; H2O / 22 h / Heating View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 11 p. 2856 - 2876