6-甲氧基-2-甲基喹啉合成路线 (共 51 条)
反应条件
phospho-tungstic acid; phosphotungstic acid; silica gel Doebner-Miller reaction; 0.166667 h; microwave irradiation;
参考文献
Sivaprasad, Ganesabaskaran; Rajesh, Rengasamy; Perumal, Paramasivan T.
Tetrahedron Letters, 2006 , vol. 47, # 11 p. 1783 - 1785
反应条件
1: H2; HOAc / Pd/C / ethanol 2: NH2OH*HCl; pyridine / ethanol 3: 86 percent / (CF3CO)2O; 4-chloranil / CH2Cl2 / 21 h / 20 °C View Scheme
参考文献
Synthesis, , # 15 p. 2415 - 2426
反应条件
1: 73 percent / H2; HOAc / Pd/C / ethanol / 24 h 2: 44 percent / NH2OH*HCl; pyridine / ethanol / 24 h 3: 83 percent / (CF3CO)2O; 4-chloranil / CH2Cl2 / 22 h / 20 °C View Scheme
参考文献
Synthesis, , # 15 p. 2415 - 2426
反应条件
1: aq. NaOH 2: H2; HOAc / Pd/C / ethanol 3: NH2OH*HCl; pyridine / ethanol 4: 86 percent / (CF3CO)2O; 4-chloranil / CH2Cl2 / 21 h / 20 °C View Scheme
参考文献
Synthesis, , # 15 p. 2415 - 2426
反应条件
1: 82 percent / aq. NaOH / 1 h 2: 73 percent / H2; HOAc / Pd/C / ethanol / 24 h 3: 44 percent / NH2OH*HCl; pyridine / ethanol / 24 h 4: 83 percent / (CF3CO)2O; 4-chloranil / CH2Cl2 / 22 h / 20 °C View Scheme
参考文献
Synthesis, , # 15 p. 2415 - 2426
反应条件
N-doped TiO2 in water T=20°C; 3 h; UV-irradiationInert atmosphere;
参考文献
Applied Catalysis A: General, , vol. 413-414, p. 213 - 222
反应条件
hydrogenchloride; aluminium trichloride
参考文献
DE24317 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 1, p. 187
反应条件
trifluorormethanesulfonic acid; 5A molecular sieve; chloranil; [NBu4][ReO4] in dichloromethane 2 h; Heating;
参考文献
Chemistry Letters, , # 1 p. 5 - 6
反应条件
ruthenium trichloride; tributylphosphine; MgBr2*Et2O in 1,3,5-trimethyl-benzene 16 h; Inert atmosphereReflux;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 2 p. 610 - 615
反应条件
chloranil in dichloromethane T=20°C; 21 h;
参考文献
Kitamura, Mitsuru; Yoshida, Masayuki; Kikuchi, Takashi; Narasaka, Koichi
Synthesis, 2003 , # 15 p. 2415 - 2426