6-甲氧基-2-甲基喹啉合成路线 (共 51 条)
参考文献
DE24317 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 1, p. 187
参考文献
Zhurnal Obshchei Khimii, , vol. 6, p. 1346
Chem. Zentralbl., , vol. 108, # I p. 4101
反应条件
[Ni0(1,5-cyclooctadiene)2]; 1,1,3,3-tetramethyldisiloxane; tri-cyclo-hexyl-phosphine in toluene T=110°C; 14 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 132, # 49 p. 17352 - 17353
反应条件
1: SeO2 / dioxane / Heating 2: H2O2; HCO2H View Scheme
参考文献
Campbell et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1844
反应条件
1: 82 percent / CH2Cl2 / 1 h / Ambient temperature 2: 61 percent / potassium carbonate / ethanol / 8 h / Ambient temperature 3: 48 percent / benzene / Irradiation 4: 63 percent / 10 percent HCl / methanol / 2 h / Ambient temperature 5: 45 percent / 10 percent HCl / methanol / 2 h / 50 °C View Scheme
参考文献
Tsuchiya; Okajima; Enkaku; Kurita
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 10 p. 3757 - 3763
反应条件
sodium hydroxide in water; hydrogen bromide
参考文献
Recordati S.A.
Patent: US2003/162777 A1, 2003 ;
US 20030162777 A1
反应条件
selenium(IV) oxide in para-xylene
16 h; Inert atmosphereReflux;
参考文献
NATIONAL HEALTH RESEARCH INSTITUTES; TAIPEI MEDICAL UNIVERSITY
Patent: US2011/275643 A1, 2011 ;
Location in patent: Page/Page column 12 ;
反应条件
C26H29ClIrNO3; hydrogen in 2,2,2-trifluoroethanol
T=40°C; P=760.051 Torr; 3 h;
参考文献
Wu, Jianjun; Barnard, Jonathan H.; Zhang, Yi; Talwar, Dinesh; Robertson, Craig M.; Xiao, Jianliang
Chemical Communications, 2013 , vol. 49, # 63 p. 7052 - 7054
反应条件
N-bromosuccinmide in acetonitrile
T=0 - 20°C; 6.5 h;
参考文献
WYETH
Patent: WO2004/24734 A1, 2004 ;
Location in patent: Page 42 ;
WO 2004/024734 A1
反应条件
in acetonitrile
T=0 - 20°C; 6.5 h;
参考文献
WYETH
Patent: WO2004/24730 A1, 2004 ;
Location in patent: Page 43 ;
WO 2004/024730 A1