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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
庚基苯
合成路线
（共 107 条）
629-04-9
1-溴代庚烷
+
98-80-6
苯硼酸
→
反应条件
1078-71-3
庚基苯
反应条件
potassium tert-butylate; palladium diacetate; di-tert-butylmethylphosphonium tetraphenylborate in 1,1-dimethylpropan-1-ol T=25°C; 24 h; Product distribution / selectivity;
参考文献
HOKKO CHEMICAL INDUSTRY CO. LTD.
Patent: EP1688424 A1, 2006 ;
Location in patent: Page/Page column 78 ;
629-04-9
1-溴代庚烷
+
2996-92-1
苯基三甲氧基硅烷
→
反应条件
1078-71-3
庚基苯
反应条件
tetrabutyl ammonium fluoride; di-tert-butylmethylphosphonium tetraphenylborate; palladium (II) bromide in tetrahydrofuran T=25°C; 21 h; Product distribution / selectivity;
参考文献
HOKKO CHEMICAL INDUSTRY CO. LTD.
Patent: EP1688424 A1, 2006 ;
Location in patent: Page/Page column 94 ;
100-59-4
苯基氯化镁
→
反应条件
1078-71-3
庚基苯
反应条件
1: 1-n-heptylbromide With P(t-Bu)2Me; palladium dichloride in tetrahydrofuran T=22°C; 0.5 h; In argon atmosphere; 2: phenyl-magnesium chloride in tetrahydrofuran T=30°C; 1.66667 h; Product distribution / selectivity;
参考文献
HOKKO CHEMICAL INDUSTRY CO. LTD.
Patent: EP1688424 A1, 2006 ;
Location in patent: Page/Page column 79 ;
108-90-7
氯苯
→
反应条件
1078-71-3
庚基苯
反应条件
1: n-heptylzinc chloride With palladium diacetate; tri-tert-butylphosphonium tetraphenylborate in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=25°C; 1 h; 2: chlorobenzene in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=120°C; 16 h; Product distribution / selectivity;
参考文献
HOKKO CHEMICAL INDUSTRY CO. LTD.
Patent: EP1688424 A1, 2006 ;
Location in patent: Page/Page column 81 ;
19969-03-0
→
反应条件
1078-71-3
庚基苯
反应条件
2,2-dimethyl-propanol; o-nitrobenzenesulfonyl hydrazide; triphenylphosphine; diethylazodicarboxylate in various solvent(s)
参考文献
Myers; Movassaghi; Zheng
Journal of the American Chemical Society, 1997 , vol. 119, # 36 p. 8572 - 8573
19969-04-1
→
反应条件
1078-71-3
庚基苯
反应条件
polymethylhydrosiloxane; tris(pentafluorophenyl)-borane in dichloromethane T=20°C;
参考文献
Chandrasekhar; Raji Reddy, Ch.; Nagendra Babu
Journal of Organic Chemistry, 2002 , vol. 67, # 25 p. 9080 - 9082
637-59-2
1-溴-3-苯基丙烷
+
92273-73-9
丁基溴化锌
→
反应条件
1078-71-3
庚基苯
反应条件
4,5-dihydroimidazolium NHC ligand; tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=20°C; Negishi cross-coupling; 24 h;
参考文献
Hadei, Niloufar; Kantchev, Eric Assen B.; O'Brien, Christopher J.; Organ, Michael G.
Journal of Organic Chemistry, 2005 , vol. 70, # 21 p. 8503 - 8507
4282-40-0
1-碘庚烷
+
100-58-3
溴化苯基镁
→
反应条件
1078-71-3
庚基苯
反应条件
1: phenyl-magnesium bromide With zinc(II) chloride in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 2: With methyl-magnesium chloride in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: 1-iodo-n-heptane With triphenylphosphine; nickel dichloride in tetrahydrofuran T=0 - 20°C; 1 h; Inert atmosphere; regioselective reaction;
参考文献
Pekel, Oezgen Oemuer; Erdik, Ender
Tetrahedron Letters, 2011 , vol. 52, # 52 p. 7087 - 7090
1671-75-6
苯庚酮
→
反应条件
1078-71-3
庚基苯
反应条件
sodium ethanolate; hydrazine hydrate T=180°C;
参考文献
Chemische Berichte, , vol. 72, p. 1893,1894
122-56-5
三正丁基硼
+
637-59-2
1-溴-3-苯基丙烷
→
反应条件
1078-71-3
庚基苯
反应条件
potassium tert-butylate; 3-Cl-pyridine-Pd-{CH-[N-(2,6-di-iPr-C6H3)-CH]2}Cl2 in isopropyl alcohol T=20°C; Suzuki cross-coupling reaction; 0.0833333 h;
参考文献
O'Brien, Christopher J.; Kantchev, Eric Assen B.; Valente, Cory; Hadei, Niloufar; Chass, Gregory A.; Lough, Alan; Hopkinson, Alan C.; Organ, Michael G.
Chemistry - A European Journal, 2006 , vol. 12, # 18 p. 4743 - 4748
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