1,4-双(二甲基氯甲硅烷基)苯合成路线 （共 12 条）
反应条件
magnesium; p-bromophenyl bromide in tetrahydrofuran T=20 - 72°C; Heating / reflux;
参考文献
Nguyen, Binh T.
Patent: US2003/233005 A1, 2003 ;
Location in patent: Page 3 ;
反应条件
acetyl chloride T=80°C; 6 h;
参考文献
Mao, Shane S. H.; Liu, Feng-Quan; Tilley, T. Don
Journal of the American Chemical Society, 1998 , vol. 120, # 6 p. 1193 - 1206
反应条件
TeCl4 in benzene 2 h; Heating;
参考文献
Chadha, Raj K.; Drake, John E.; Neo, Mary K. H.
Journal of Organometallic Chemistry, 1984 , vol. 277, # 1 p. 47 - 52
反应条件
bis(benzonitrile)palladium(II) dichloride; triphenylphosphine 1.) 145 deg C, 24 h; 2.) 175 deg C, 48 h;
参考文献
Rich, Jonathan D.
Journal of the American Chemical Society, 1989 , vol. 111, # 15 p. 5886 - 5893
反应条件
1: 63 percent / Mg / tetrahydrofuran / 8 h / Heating 2: 98 percent / AcCl / 6 h / 80 °C View Scheme
参考文献
Moores, Audrey; Defieber, Christian; Mezailles, Nicolas; Maigrot, Nicole; Ricard, Louis; Le Floch, Pascal
New Journal of Chemistry, 2003 , vol. 27, # 6 p. 994 - 999
反应条件
1: p-bromophenyl bromide With magnesium in tetrahydrofuran 2: dimethyl-dichlorosilane in tetrahydrofuran T=0°C; 1 h;
参考文献
Beyer, Christian; Boehme, Uwe; Pietzsch, Claus; Roewer, Gerhard
Journal of Organometallic Chemistry, 2002 , vol. 654, # 1-2 p. 187 - 201
参考文献
Gmelin Handbook: Si: MVol.C, 67, page 185 - 187
参考文献
Moores, Audrey; Defieber, Christian; Mezailles, Nicolas; Maigrot, Nicole; Ricard, Louis; Le Floch, Pascal
New Journal of Chemistry, 2003 , vol. 27, # 6 p. 994 - 999
参考文献
Du Pont de Nemours and Co.
Patent: US2562000 , 1946 ;
反应条件
sodium hydroxide in sodium hydroxide; diethyl ether (CH3)2ClSiC6H4SiCl(CH3)2 and equival. amt. of aq. NaOH in ether at about 0°C;; crystn. from ether or by addn. of C6H6 to the ether soln.;;
参考文献
Gmelin Handbook: Si: MVol.C, 88, page 240 - 242
