1: (R)-2,2'-bis(trifluoromethanesulfonyloxy)-1,1'-binaphthalene With Cl2Ni(1,2-bis(diphenylphosphino)ethane) in N,N-dimethyl-formamide 2: diphenylphosphinous bromide With 1,4-diaza-bicyclo[2.2.2]octane in N,N-dimethyl-formamide T=110°C;
参考文献
Chemistry - A European Journal, , vol. 17, # 39 p. 10828 - 10831
in chloroform-d1
1.) 20 deg C, 2 h, 2.) 100 deg C , 2 h;
参考文献
Michie, Jacqui; Miller, J. Allen; Nunn, M. John; Stewart, Denis
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1744 - 1749
in chloroform-d1
20 deg C -> 150 deg C, dark; reactions of aromatic aldehydes with PBr3, PI3, and Ph2PBr; Product distribution;
参考文献
Michie, Jacqui; Miller, J. Allen; Nunn, M. John; Stewart, Denis
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1744 - 1749
1: Et3N / benzene / 24 h
2: 56 percent / CH2Cl2
3: 84 percent / HCl; water / CH2Cl2 / 72 h / 20 °C
View Scheme
参考文献
Kostyuk, Alexandr N.; Svyaschenko, Yurii V.; Volochnyuk, Dmitriy M.; Lysenko, Nikolai V.; Tolmachev, Andrei A.; Pinchuk, Alexandr M.
Tetrahedron Letters, 2003 , vol. 44, # 34 p. 6487 - 6491
