1: N-methylaniline With n-butyllithium in tetrahydrofuran T=-70°C; Inert atmosphere; 2: With carbon dioxide in tetrahydrofuran T=0 - 10°C; Inert atmosphere; 3: chloro-diphenylphosphine Further stages;
参考文献
Lightburn, Thomas E.; Dombrowski, Michael T.; Tan, Kian L.
Journal of the American Chemical Society, 2008 , vol. 130, # 29 p. 9210 - 9211
1: 1.) -5 - 5deg C, 2.) room temp. 2: CH2Cl2 / 4 h / 90 - 120 °C 3: NH2NH2 hydrate / 40 - 60 °C View Scheme
参考文献
Razumov, A. I.; Tarasova, R. I.; Mikheeva, A. S.; Nikolaeva, N. G.; Yafarova, R. L.
J. Appl. Chem. USSR (Engl. Transl.), 1983 , vol. 56, # 2 p. 342 - 344,325 - 327
Razumov, A. I.; Tarasova, R. I.; Mikheeva, A. S.; Nikolaeva, N. G.; Yafarova, R. L.
J. Appl. Chem. USSR (Engl. Transl.), 1983 , vol. 56, # 2 p. 342 - 344,325 - 327
