反应条件
1: 1,3-dimethoxy benzene With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; diethyl ether
T=0°C; 1.5 h; Inert atmosphereSchlenk technique;
2: chloro-diphenylphosphine in tetrahydrofuran; diethyl ether
T=-50 - 20°C; Inert atmosphereSchlenk technique;
参考文献
Richard, Vincent; Ipouck, Melinda; Merel, Delphine S.; Gaillard, Sylvain; Whitby, Richard J.; Witulski, Bernhard; Renaud, Jean-Luc
Chemical Communications, 2014 , vol. 50, # 5 p. 593 - 595
