1: 4-bromo-pyridine With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; diethyl ether; pentane
T=-115°C; Inert atmosphere;
2: chloro-diphenylphosphine in tetrahydrofuran; diethyl ether; pentane
T=-70°C; Inert atmosphere;
参考文献
Goudriaan, P. Elsbeth; Jang, Xiao-Bin; Kuil, Mark; Lemmens, Renske; Van Leeuwen, Piet W. N. M.; Reek, Joost N. H.
European Journal of Organic Chemistry, 2008 , # 36 p. 6079 - 6092
tetra-n-butylammonium tetrafluoroborate; tetra-(n-butyl)ammonium iodide in various solvent(s)
Ambient temperatureelektrochemical reaction, anode Mg bar, cathode stainless steel; var. solv.; Yields of byproduct given;
参考文献
Folest, J. C.; Nedelec, J. Y.; Perichon, J.
Tetrahedron Letters, 1987 , vol. 28, # 17 p. 1885 - 1886
1: 2,2'-Dibromodiphenylamine With n-butyllithium in diethyl ether; hexane
T=0°C; 1.5 h;
2: chloro-diphenylphosphine in diethyl ether; hexane
T=0 - 20°C;
参考文献
Winter, Angelika M.; Eichele, Klaus; Mack, Hans-Georg; Potuznik, Suzan; Mayer, Hermann A.; Kaska, William C.
Journal of Organometallic Chemistry, 2003 , vol. 682, # 1-2 p. 149 - 154
