1: alpha-Terthiophene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 1 h;
2: chloro-diphenylphosphine in tetrahydrofuran; hexane
T=25°C; 0.5 h; Further stages.;
参考文献
Clot; Wolf; Patrick
Journal of the American Chemical Society, 2001 , vol. 123, # 41 p. 9963 - 9973
1: 5-bromo-lt;2,2',5',2''gt;-terthiophene With magnesium; ethylene dibromide in tetrahydrofuran
T=20°C; 1 h; sonication;
2: chloro-diphenylphosphine in diethyl ether; hexane
T=20°C; 1 h; Further stages.;
参考文献
Field, John S.; Haines, Raymond J.; Lakoba, Elena I.; Sosabowski, M. Hal
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 24 p. 3352 - 3360