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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
异戊酰氯
合成路线
（共 214 条）
108-12-3
异戊酰氯
→
反应条件
919516-14-6
反应条件
1: 52 percent / Li2MnCl4 / tetrahydrofuran; diethyl ether / 1.5 h / 0 - 20 °C 2: 71 percent / anhydrous cerium(III) chloride / tetrahydrofuran / 20 °C 3: 52 percent / potassium hydrogen sulfate / 3 h / 110 °C / 180.01 Torr View Scheme
参考文献
Kraft, Philip; Popaj, Kasim
Tetrahedron, 2006 , vol. 62, # 52 p. 12211 - 12219
108-12-3
异戊酰氯
→
反应条件
919516-22-6
反应条件
1.1: 53 percent / Li2MnCl4 / tetrahydrofuran; diethyl ether / 1.5 h / 0 - 20 °C 2.1: 68 percent / anhydrous cerium(III) chloride / tetrahydrofuran / 20 °C 3.1: 54 percent / potassium hydrogen sulfate / 3 h / 110 °C / 180.01 Torr 4.1: methyl magnesium chloride / tetrahydrofuran / 2 h / Heating 4.2: 85 percent / tetrahydrofuran / Heating View Scheme
参考文献
Kraft, Philip; Popaj, Kasim
Tetrahedron, 2006 , vol. 62, # 52 p. 12211 - 12219
108-12-3
异戊酰氯
→
反应条件
919516-25-9
反应条件
1.1: 52 percent / Li2MnCl4 / tetrahydrofuran; diethyl ether / 1.5 h / 0 - 20 °C 2.1: 71 percent / anhydrous cerium(III) chloride / tetrahydrofuran / 20 °C 3.1: 52 percent / potassium hydrogen sulfate / 3 h / 110 °C / 180.01 Torr 4.1: methyl magnesium chloride / tetrahydrofuran / 2 h / Heating 4.2: 83 percent / tetrahydrofuran / Heating View Scheme
参考文献
Kraft, Philip; Popaj, Kasim
Tetrahedron, 2006 , vol. 62, # 52 p. 12211 - 12219
108-12-3
异戊酰氯
→
反应条件
919516-32-8
反应条件
1.1: 53 percent / Li2MnCl4 / tetrahydrofuran; diethyl ether / 1.5 h / 0 - 20 °C 2.1: 68 percent / anhydrous cerium(III) chloride / tetrahydrofuran / 20 °C 3.1: 54 percent / potassium hydrogen sulfate / 3 h / 110 °C / 180.01 Torr 4.1: methyl magnesium chloride / tetrahydrofuran / 2 h / Heating 4.2: 85 percent / tetrahydrofuran / Heating 5.1: 80 percent / lithium aluminum hydride / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
Kraft, Philip; Popaj, Kasim
Tetrahedron, 2006 , vol. 62, # 52 p. 12211 - 12219
108-12-3
异戊酰氯
→
反应条件
919516-34-0
反应条件
1.1: 52 percent / Li2MnCl4 / tetrahydrofuran; diethyl ether / 1.5 h / 0 - 20 °C 2.1: 71 percent / anhydrous cerium(III) chloride / tetrahydrofuran / 20 °C 3.1: 52 percent / potassium hydrogen sulfate / 3 h / 110 °C / 180.01 Torr 4.1: methyl magnesium chloride / tetrahydrofuran / 2 h / Heating 4.2: 83 percent / tetrahydrofuran / Heating 5.1: 81 percent / lithium aluminum hydride / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
Kraft, Philip; Popaj, Kasim
Tetrahedron, 2006 , vol. 62, # 52 p. 12211 - 12219
108-12-3
异戊酰氯
→
反应条件
922177-82-0
反应条件
1: benzene / 12 h / 20 °C 2: 2.3139 g / 3.5 h / 260 - 280 °C / 0.4 Torr 3: 48 percent / tetrahydrofuran / 1.5 h / cooling 4: 93 percent / KOH / methanol; H2O / 7 h / Heating View Scheme
参考文献
Green, James R.; Majewski, Marek; Snieckus, Victor
Canadian Journal of Chemistry, 2006 , vol. 84, # 10 p. 1397 - 1410
689-97-4
乙烯基乙炔
+
108-12-3
异戊酰氯
→
反应条件
94694-68-5
+
94694-65-2
反应条件
aluminium trichloride in dichloromethane T=-20°C; 0.25 h; Product distribution;
参考文献
Melikyan, G. G.; Babayan, E. V.; Atanesyan, K. A.; Badanyan, Sh. O.
Journal of Organic Chemistry USSR (English Translation), 1984 , p. 1884 - 1889
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 10 p. 2067 - 2072
13170-43-9
(三甲基硅基)甲基氯化镁
+
108-12-3
异戊酰氯
→
反应条件
95547-15-2
反应条件
copper(l) iodide in diethyl ether -78 deg C up to 0 deg C;
参考文献
Yamamoto, Yohsuke; Ohdoi, Keisuke; Nakatani, Masayuki; Akiba, Kin-ya
Chemistry Letters, 1984 , p. 1967 - 1968
108-12-3
异戊酰氯
→
反应条件
478-67-1
4-丙基-5,7-二羟基-6-(3-甲基丁酰基)-8-(3-甲基-2-丁烯基)-2H-1-苯并吡喃-2-酮
反应条件
1: 80 percent / AlCl3 / CS2; nitrobenzene / 0.5 h / Heating 2: cc. H2SO4 / acetic acid / 240 h / Ambient temperature 3: 22 percent / 10percent aq. potassium hydroxide / 1.5 h / 0 °C View Scheme
参考文献
Crombie; Jones; Palmer
Tetrahedron Letters, 1985 , vol. 26, # 24 p. 2929 - 2932
108-12-3
异戊酰氯
→
反应条件
5032-03-1
反应条件
2: AlCl3 / 165 °C 3: Zn-Hg, aq. HCl / ethanol View Scheme
参考文献
Bonner,W.A.; De Graw,J.I.
Tetrahedron, 1962 , vol. 18, p. 1295 - 1309
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