lithium butanide in diethyl ether; hexane addn. of soln. of i-Pr2NH in ether and soln. of Li-butanide in hexane at 20°C to B-compound at 0°C, stirred for 2 h at room temp.; filtration, removal of solvent, recrystn. from hexane at -70°C; elem. anal.;
参考文献
Bonn, Karl-Heinz van; Schreyer, Peter; Paetzold, Peter; Boese, Roland
Chemische Berichte, 1988 , vol. 121, p. 1045 - 1058
in toluene under N2 or Ar; soln. of amine (excess) satd. with CO2 at room temp., then Mn(cp)2 added, mixture stirred for 16 h,; attempts of recrystn. failed due to high soly. of Mn-complex even in aliphatic hydrocarbons, elem. anal., elem. anal.;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 2921 - 2926
in 1,4-dioxane; water T=25°C; solvent isotope effect (kH/kD); Rate constant;
参考文献
Garcia-Rio, Luis; Iglesias, Emilia; Leis, J. Ramon; Pena, M. Elena; Rios, Ana
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 1 p. 29 - 37
dibutyltin dibenzoate in benzene T=25°C; various times; Rate constantKinetics;
参考文献
Litvinenko, L. M.; Oleinik, N. M.; Garkusha-Bozhko, I. P.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 11 p. 2056 - 2061
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 11 p. 2353 - 2358
