manganese(III) porphyrin; iodosylbenzene in dichloromethane
T=0°C; 2 h;
参考文献
Larsen, Jan; Joergensen, Karl Anker
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 8 p. 1213 - 1217
Borthakur, R. C.; Borthakur, N.; Rastogi, R. C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 3 p. 244 - 248
in toluene
stirring of the boroxine with diisopropylamine in toluene at room temp.for 15 h; heating at 70°C for 1 h;; filtration; evapn. of the filtrate; drying under vac.; recrystn. from benzene; elem. anal.;;
