1: 1-bromo-3-chlorobenzene; diisopropylamine With n-butyllithium in tetrahydrofuran; hexane 3 h; 2: methyl chloroformate in tetrahydrofuran T=-78°C; 1.25 h;
参考文献
Hickey, Matthew R.; Allwein, Shawn P.; Nelson, Todd D.; Kress, Michael H.; Sudah, Osama S.; Moment, Aaron J.; Rodgers, Stephen D.; Kaba, Mahmoud; Fernandez, Paul
Organic Process Research and Development, 2005 , vol. 9, # 6 p. 764 - 767