phosphorus pentachloride in neat (no solvent) 1.) 110-120 deg C, 1 h, 2.) room temp., 2.5 h then 90 deg C, 3 h; Title compound not separated from byproducts;
参考文献
Mahajan; Araujo
Canadian Journal of Chemistry, 1987 , vol. 65, # 1 p. 224 - 225
Shuikin,N.I. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1961 , p. 1010 - 1013
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1961 , # 6 p. 1094 - 1098
