ruthenium trichloride; triphenylphosphine; tin(ll) chloride in 1,4-dioxane; acetone T=180°C; Condensation; 20 h; Title compound not separated from byproducts;
参考文献
Cho, Chan Sik; Oh, Byoung Ho; Shim, Sang Chul
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 5 p. 1175 - 1178
1: 0.75 h / 110 °C 2: diphenylether / 0.5 h / |Reflux 3: sodium hydroxide / water / 0.5 h / |Reflux 4: diphenylether / 0.75 h / |Reflux 5: trichlorophosphate / 1 h / 140 °C View Scheme
参考文献
Nsumiwa, Samkele; Kuter, David; Wittlin, Sergio; Chibale, Kelly; Egan, Timothy J.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 13 p. 3738 - 3748