KOH in tetrahydrofuran byproducts: KCl; Ga-compds. in THF stirred for 30 h at room temp., addn. of KOH, stirred for 5 days at room temp. under inert atmosphere; filtered, filtrate evapd., washed with hexane, crystn. (THF);
参考文献
Storre, Jens; Belgardt, Thomas; Stalke, Dietmar; Roesky, Herbert W.
Angewandte Chemie, 1994 , vol. 106, p. 1365 - 1366
H2O in toluene soln. of Ga-compd. in toluene at -78°C splashed with water, slowly warmed to room temp. under stirring, stirred for 3 d; evapn. of volatile components in vac., washed with hexane, dried (15 h, vac.);
参考文献
Storre, Jens; Belgardt, Thomas; Stalke, Dietmar; Roesky, Herbert W.
Angewandte Chemie, 1994 , vol. 106, p. 1365 - 1366
in chloroform; water mixt. of aryl(m-carboran-9-yl)iodonium tetrafluoroborate, NaF, water and chloroform was vigorously stirred under reflux at 56°C, 2.5 h; internal standard (chlorobenzene) added and org. layer was analysed by GLC;
