1-氨基-3,5-二甲苯合成路线 （共 187 条）
反应条件
sulfuric acid; nitric acid T=0°C;
参考文献
Bamberger
Justus Liebigs Annalen der Chemie, 1925 , vol. 443, p. 205
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Ibbotson; Kenner
Journal of the Chemical Society, 1923 , vol. 123, p. 1268
反应条件
sulfuric acid; nitric acid
参考文献
Noelting; Forel
Chemische Berichte, 1885 , vol. 18, p. 2677,2681
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=20°C; 5 h; Inert atmosphere;
参考文献
Hwang, Soonho; Choi, Sang Yoon; Lee, Jin Hee; Kim, Shinae; In, Jinkyung; Ha, Sang Keun; Lee, Eunjung; Kim, Tae-Yoon; Kim, Sun Yeou; Choi, Sun; Kim, Sanghee
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 15 p. 5602 - 5609
反应条件
1: 1. conc. hydrochloric acid, NaNO2; / 1. 0 degC, 30min.; 2. 45 degC 2: 92 percent / LiAlH4 / diethyl ether / 3 h / Heating 3: 82 percent / NaOH / aq. ethanol / r.t., 30min., then reflux, 4h 4: 78 percent / polyphosphoric acid / 1.5 h / 190 - 200 °C 5: 71 percent / Se powder / 8 h / 300 °C View Scheme
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1485 - 1495
反应条件
hydrogenchloride beim Erhitzen des Reaktionsprodukts mit Ca(OH)2;
参考文献
Luening
Acta Chemica Scandinavica (1947-1973), 1959 , vol. 13, p. 1623,1630
参考文献
Luening
Acta Chemica Scandinavica (1947-1973), 1959 , vol. 13, p. 1623,1630
反应条件
boric acid in toluene 18 h; Heating;
参考文献
Anderson, Joanne; Davis, Roman; Fitzgerald, Russ; Haberman, Jannine
Synthetic Communications, 2006 , vol. 36, # 15 p. 2129 - 2133
反应条件
in xylene 3 h; Heating;
参考文献
Thevis, Mario; Krug, Oliver; Schaenzer, Wilhelm
Journal of Mass Spectrometry, 2006 , vol. 41, # 3 p. 332 - 338
反应条件
indium(III) chloride in acetonitrile T=20°C; 2 h; diastereoselective reaction;
参考文献
Chemistry - A European Journal, , vol. 18, # 16 p. 5056 - 5063
反应条件
1: ethanol / 3 h / Reflux 2: indium(III) chloride / acetonitrile / 2 h / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 18, # 16 p. 5056 - 5063
