反应条件
1: conc. H2SO4 / 2 h / 90 °C 2: 16 percent / AlCl3 / nitrobenzene; CS2 3: 93 percent / pyridine / toluene / 144 h / Heating 4: 30 percent / pyridinium tosylate, TFA, pyridine / 4 h / 140 °C 5: 1.) CeCl3(H2O)7, 2.) NaBH4 / 1.) EtOH, RT, 1.5 h, 2.) EtOH, -30 deg C, 8.5 h View Scheme
参考文献
Flavin, Michael T.; Rizzo, John D.; Khilevich, Albert; Kucherenko, Alla; Sheinkman, Abram K.; Vilaychack, Vilayphone; Lin, Lin; Chen, Wei; Greenwood, Eugenia Mata; Pengsuparp, Thitima; Pezzuto, John M.; Hughes, Stephen H.; Flavin, Thomas M.; Cibulski, Michael; Boulanger, William A.; Shone, Robert L.; Xu, Ze-Qi
Journal of Medicinal Chemistry, 1996 , vol. 39, # 6 p. 1303 - 1313
