反应条件
1: NH3, HCl 2: 1.) cc. HCl, NaNO2; 2.) NaN3 / 1.) H2O, 0 deg C, 10 min; 2.) H2O, 0 deg C, 40 min 3: 1.) NaH / 1.) DMF, 25 deg C, 1 h; 2.) DMF, 25 deg C, 1 h 4: 90 percent / K2CO3 / 1,2-dimethoxy-ethane / 2 h / 80 °C View Scheme
参考文献
Richardson, Stewart K.; Jeganathan, Alwarsamy; Mani, Rajarathnam S.; Haley, Boyd E.; Watt, David S.; Trusal, Lynn R.
Tetrahedron, 1987 , vol. 43, # 13 p. 2925 - 2934
