1,3,5-三甲基己羟基-1,3,5-三嗪合成路线 (共 63 条)
反应条件
T=150 - 200°C; nitrogen atmosphere;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 54, # 3 p. 635 - 640,562 - 566
参考文献
Journal fur Praktische Chemie - Chemiker - Zeitung, , vol. 338, # 1 p. 47 - 50
反应条件
in chloroform-d1 in an NMR tube, after 6 days at room temp., conversion was ca. 20 percent, further 5 days at 75 °C, conversion increased up to 35 percent; detected by NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 600, # 1-2 p. 71 - 83
反应条件
in chloroform-d1 in an NMR tube, 7 days at room temp. (50 percent conversion), after 24 h heating at 75 .degre.C the reaction was complete; detected by NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 600, # 1-2 p. 71 - 83
反应条件
in chloroform-d1 in an NMR tube, after 6 days at room temp., conversion was ca. 20 percent, further 5 days at 75 °C, conversion increased up to 35 percent; detected by NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 600, # 1-2 p. 71 - 83
反应条件
in chloroform-d1 in an NMR tube, over 14 days at room temp. and after heating at 75 .degre.C for other 14 days; detected by NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 600, # 1-2 p. 71 - 83
反应条件
in chloroform-d1 in an NMR tube, 7 days at room temp. (50 percent conversion), after 24 h heating at 75 .degre.C the reaction was complete; detected by NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 600, # 1-2 p. 71 - 83
反应条件
in chloroform-d1 in an NMR tube, over 14 days at room temp. and after heating at 75 .degre.C for other 14 days; detected by NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 600, # 1-2 p. 71 - 83
反应条件
T=450°C; P=24 Torr; other temperature; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 58, # 19 p. 5067 - 5075
反应条件
1) 10 h, rt, 2) 30 min, reflux;
参考文献
Angewandte Chemie, , vol. 102, # 8 p. 917 - 919