1,3,5-三甲基己羟基-1,3,5-三嗪合成路线 (共 63 条)
反应条件
T=195 - 200°C; auf 260graderhitzten Dampfes;
参考文献
Southern Prod.Co.
Patent: US2657237 , 1948 ;
反应条件
T=80 - 90°C; Hydrogenation;
参考文献
Southern Prod.Co.
Patent: US2657237 , 1948 ;
参考文献
Graymore
Journal of the Chemical Society, 1931 , p. 1490,1492
反应条件
chloro-trimethyl-silane in toluene; acetonitrile Heating / reflux; Product distribution / selectivity;
参考文献
WO2005/37822 A1, ;
Page/Page column 11 ;
反应条件
hydrogenchloride T=225°C; 0.25 h; Mechanism;
参考文献
D'Silva, Themistocles D. J.; Lopes, Anibal
Journal of the Chemical Society, Chemical Communications, 1986 , # 10 p. 795 - 796
反应条件
nitric acid in acetic acid T=5 - 75°C;
参考文献
Fischer, Niko; Karaghiosoff, Konstantin; Klapoetke, Thomas M.; Stierstorfer, Joerg
Zeitschrift fur Anorganische und Allgemeine Chemie, 2010 , vol. 636, # 5 p. 735 - 749
反应条件
zinc(II) chloride in dichloromethane T=135°C; 1 h;
参考文献
Prishchenko; Livantsov; Novikova; Livantsova; Koval'; Grigor'ev
Russian Journal of General Chemistry, 2004 , vol. 74, # 9 p. 1317 - 1320
反应条件
1.) CHCl3, r.t., 1 h, 2.) CHCl3, r.t.; Yield given. Multistep reaction;
参考文献
Ikeda, Kiyoshi; Morimoto, Toshiaki; Sekiya, Minoru
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 4 p. 1178 - 1182
反应条件
triethylamine in diethyl ether
T=-50°C; 0.5 h;
参考文献
Anikin, O. V.; Chlenov, I. E.; Tartakovskii, V. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 1.2 p. 200 - 202
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 1 p. 217 - 219
反应条件
zinc(II) chloride in dichloromethane
T=135°C; 1 h;
参考文献
Prishchenko; Livantsov; Novikova; Livantsova; Koval'; Grigor'ev
Russian Journal of General Chemistry, 2004 , vol. 74, # 9 p. 1317 - 1320