2,4,6-三甲基吡啶合成路线 (共 205 条)
反应条件
lithium; benzonitrile 1.) diethyl ether, reflux, 1 h, 2.) ether, reflux, 2.5 h, 3.) ether; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Compagnon, Paul-Louis; Gasquez, Francoise; Kimny, Tan
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 1 p. 57 - 64
反应条件
lithium 1.) diethyl ether, reflux, 1 h, 2.) ether, reflux, 2.5 h, 3.) ether; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Compagnon, Paul-Louis; Gasquez, Francoise; Kimny, Tan
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 1 p. 57 - 64
反应条件
lithium 1.) diethyl ether, reflux, 1 h, 2.) ether, reflux, 2.5 h, 3.) ether; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Compagnon, Paul-Louis; Gasquez, Francoise; Kimny, Tan
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 1 p. 57 - 64
反应条件
lithium 1.) diethyl ether, reflux, 1 h, 2.) ether, reflux, 2.5 h, 3.) ether; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Compagnon, Paul-Louis; Gasquez, Francoise; Kimny, Tan
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 1 p. 57 - 64
反应条件
lithium 1.) diethyl ether, reflux, 1 h, 2.) ether, reflux, 2.5 h, 3.) ether; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Compagnon, Paul-Louis; Gasquez, Francoise; Kimny, Tan
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 1 p. 57 - 64
反应条件
lithium 1.) diethyl ether, reflux, 1 h, 2.) ether, reflux, 2.5 h, 3.) ether; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Compagnon, Paul-Louis; Gasquez, Francoise; Kimny, Tan
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 1 p. 57 - 64
反应条件
T=190°C; anschliessend Erhitzen mit wss.-methanol. KOH;
参考文献
Wilds; Meader
Journal of Organic Chemistry, 1948 , vol. 13, p. 763,773
反应条件
1: 85 percent / HNO3 / 1.5 h / 0 - 20 °C 2: 95 percent / H2 / Pd/C / 2585.74 Torr View Scheme
参考文献
Plazek
Chemische Berichte, 1939 , vol. 72, p. 577,579
反应条件
phosphonitrilic chloride trimer; dihydrogen peroxide T=25°C; Neat (no solvent); chemoselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 75, # 18 p. 6208 - 6213
反应条件
N-bromosuccinmide; Petroleum ether unter der Einwirkung von UV-Licht; ueber mehrere Stufen;
参考文献
Redel; Gauthier
Bulletin de la Societe Chimique de France, 1948 , p. 607,610
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Buisman; Stevens; van der Vliet
Recueil des Travaux Chimiques des Pays-Bas, 1947 , vol. 66, p. 83,89
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Glaxo Labor. Ltd.
Patent: US2468859 , 1947 ;
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Hartford Nation. Bank and Trust Co.
Patent: US2441091 , 1946 ;
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Giacomello
Ricerca Scientifica, 1946 , vol. 26, p. 1653
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Bernstein et al.
Journal of Organic Chemistry, 1949 , vol. 14, p. 433,437, 443