2,4,6-三甲基吡啶合成路线 (共 205 条)
反应条件
chromium(VI) oxide; sulfuric acid
T=0 - 75°C; 27 h;
参考文献
Gryko, Dorota; Gryko, Daniel T.; Sierzputowska-Gracz, Hanna; Piatek, Piotr; Jurczak, Janusz
Helvetica Chimica Acta, 2004 , vol. 87, # 1 p. 156 - 166
反应条件
air; vanadium(V)-oxide-molybdenum (VI)-oxide silica gel-catalyst; water
T=380°C;
参考文献
Mathes; Sauermilch
Chemische Berichte, 1955 , vol. 88, p. 1276,1281
反应条件
β-VO(PO3)2 in gas
T=400°C; selectivity of reaction, rates of partial and total oxidation; Product distributionRate constant;
参考文献
Leitis, L. Ya.; Skolmeistere, R. A.; Golender, L. O.; Yansone, D. P.; Meksh, P. A.; Shimanskaya, M. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 1 p. 63 - 66
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 1 p. 75 - 79
反应条件
T=380°C; Leiten ueber mit Vanadium(V)-oxid und Molybdaen(VI)-oxid impraegniertes Silicagel;
参考文献
Mathes; Sauermilch
Chemische Berichte, 1955 , vol. 88, p. 1276,1281
反应条件
ammonium hydroxide; oxygen; vanadium pentoxide; Titanium(IV) oxide
T=300°C; Product distribution; Further Variations:Temperatures;
参考文献
Kagarlitsky; Krichevsky
Chemistry of Heterocyclic Compounds, 2003 , vol. 39, # 3 p. 315 - 317
反应条件
in ethanol
equimolar amts.; recrystn. (CH2Cl2 or Me2CO); elem. anal.;
参考文献
Meester et al.
Inorganica Chimica Acta, 1976 , vol. 16, p. 191
反应条件
in dichloromethane
byproducts: t-BuNCHCHNt-Bu;
参考文献
Poel, Henk van der; Koten, Gerard van; Stein, Gerard C. van
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1981 , p. 2164 - 2171
反应条件
in water
addn. of substituted pyridine to soln. of Pt-complex (pptn.); recrystn. (CHCl3/pentane);
参考文献
Natile, Giovanni; Maresca, Luciana; Cattalini, Lucio
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1977 , p. 651 - 655
反应条件
in dichloromethane
byproducts: Me2EtNCHCHnMe2Et;
参考文献
Poel, Henk van der; Koten, Gerard van; Stein, Gerard C. van
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1981 , p. 2164 - 2171
反应条件
sulfuryl dichloride in tetrachloromethane; toluene
参考文献
Hoechst Aktiengesellschaft
Patent: US4182773 A1, 1980 ;