1: With copper(l) iodide; lithium tert-butylate in acetonitrile
T=20°C; 0.0833333 h; Inert atmosphere;
2: in acetonitrile
T=20°C; 24 h; Inert atmosphereIrradiation;
参考文献
Do, Hien-Quang; Bachman, Shoshana; Bissember, Alex C.; Peters, Jonas C.; Fu, Gregory C.
Journal of the American Chemical Society, 2014 , vol. 136, # 5 p. 2162 - 2167
in N,N-dimethyl-formamide; acetonitrile
T=20°C; Inert atmosphere; Reagent/catalyst;
参考文献
Do, Hien-Quang; Bachman, Shoshana; Bissember, Alex C.; Peters, Jonas C.; Fu, Gregory C.
Journal of the American Chemical Society, 2014 , vol. 136, # 5 p. 2162 - 2167
potassium hydrogencarbonate in N,N-dimethyl-formamide
Ambient temperature;
参考文献
Kalgutkar, Amit S.; Kozak, Kevin R.; Crews, Brenda C.; Hochgesang Jr., G. Phillip; Marnett, Lawrence J.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 24 p. 4800 - 4818