chlorine; L type zeolite (TSZ-500KOA) in 1,2-dichloro-ethane T=70°C; 3 h; var. solvents, also reaction in the presence of oxygen; Product distribution;
potassium hydroxide; hydrogen; palladium on activated charcoal in 2,2,4-trimethylpentane T=50°C; var. cat.: Raney-Ni, add. of Aliquat 336; Product distribution;
Chesnokova, T. A.; Kornev, A. N.; Semenov, V. V.; Kurskii, Yu. A.; Razuvaev, G. A.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 5.1 p. 1057 - 1062,934 - 937
cesium fluoride in various solvent(s) 1) 20 deg C, 30 min, 2) 50 deg C, 6 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 1.2 p. 174 - 176
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 38, # 1 p. 188 - 190
in water; 1,2-dichloro-ethane T=72°C; 0.25 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, # 10 p. 2130 - 2135
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2332 - 2338
sodium bromide; sodium chloride in glycerol T=21 - 23.5°C; investigations of thermal dediazoniation in various solvents as a function of viscosity; the reaction are diffusion controlled; Product distributionKinetics;