1: chlorobenzene With AlCl3, aluminium chloride in dichloromethane
T=10 - 15°C; 1 h;
2: α-bromopropionyl bromide in dichloromethane
T=20°C; 16 h;
3: With water in dichloromethane
T=0°C;
参考文献
Botton, Gerard; Leriche, Caroline; Arbellot De Vacqueur, Annick; Audet, Annick; Gleitz, Johannes
Patent: US2010/286129 A1, 2010 ;
Location in patent: Page/Page column 21 ;