in neat (no solvent) T=140°C; 30 h; sealed ampule;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 17, # 8 p. 756 - 758
Khimiya Geterotsiklicheskikh Soedinenii, , # 8 p. 1028 - 1030
carbon monoxide in tetrahydrofuran; diethyl ether addn. of RNH2 to suspn. of complex, CO (40 bar), warmed up to 45°C, 20h, hydrolysis with H2SO4, sepn. of organic phase, dried, crystn. of organic products from hexane/CHCl3 = 20/1;
参考文献
Journal of Organometallic Chemistry, , vol. 254, # 2 p. 267 - 272