反应条件
1: C56H59N2O13P With N,O-bis(trimethylsilyl) trifluoroacetamide in dichloromethane T=0°C; 0.0333333 h; Inert atmosphere; 2: With 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane T=0°C; 0.333333 h; Inert atmosphere; 3: cyclohexylamine Further stages;
参考文献
Capolicchio, Samanta; Thakor, Divyeshsinh T.; Linden, Anthony; Jessen, Henning J.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 27 p. 6912 - 6916
Angew. Chem., 2013 , vol. 125, # 27 p. 7050 - 7054