3-(3,5-二甲氧基苯基)-1-丙醇合成路线 （共 2 条）
反应条件
oxalyl dichloride; dimethyl sulfoxide; triethylamine in dichloromethane T=-60 - 20°C; Oxidation; 2.3 h;
参考文献
Huffman, John W.; Liddle, John; Duncan Jr., Sammy G.; Yu, Shu; Martin, Billy R.; Wiley, Jenny L.
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 12 p. 2383 - 2396
反应条件
1: PBr3
2: (i) KI, aq. EtOH, (ii) KOH, pentan-1-ol
3: polyphosphoric acid
View Scheme
参考文献
Yilmaz, Sueleyman; Goeksu, Sueleyman
Synthetic Communications, 2014 , vol. 44, # 8 p. 1058 - 1065
