1-苄基-3,4-二氢-1H-吡啶-2-酮合成路线 （共 8 条）
反应条件
hydrogen; bis(triphenylphosphine)carbonylrhodium(I) chloride; triphenylphosphine in tetrahydrofuran T=100°C; P=62057.8 Torr; 40 h;
参考文献
Ojima, Iwao; Korda, Anna; Shay, William R.
Journal of Organic Chemistry, 1991 , vol. 56, # 6 p. 2024 - 2030
反应条件
hydrogen; bis(triphenylphosphine)carbonylrhodium(I) chloride; triphenylphosphine in tetrahydrofuran T=100°C; P=62057.8 Torr; 40 h;
参考文献
Ojima, Iwao; Korda, Anna
Tetrahedron Letters, 1989 , vol. 30, # 46 p. 6283 - 6286
反应条件
methanesulfonyl chloride; triethylamine in dichloromethane T=0 - 20°C; 2 h;
参考文献
Suarez Del Villar, Irene; Gradillas, Ana; Perez-Castells, Javier
European Journal of Organic Chemistry, 2010 , # 30 p. 5850 - 5862
反应条件
1: With lithium triethylborohydride in tetrahydrofuran; toluene T=-70°C; 0.5 h; 2: With 4-(N,N-dimethlyamino)pyridine; N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride in tetrahydrofuran; toluene T=-70 - 20°C; 2 h;
参考文献
Yu, Jurong; Truc, Vu; Riebel, Peter; Hierl, Elizabeth; Mudryk, Boguslaw
Tetrahedron Letters, 2005 , vol. 46, # 23 p. 4011 - 4013
反应条件
sodium hydride in tetrahydrofuran T=20°C; 12 h;
参考文献
Salanski, Piotr; Young, Kwan Ko; Lee, Kee-In
Mendeleev Communications, 2006 , # 1 p. 46 - 48
反应条件
1.1: tetrahydrofuran / 0.5 h / 20 °C 1.2: 1 h / 80 °C 2.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -78 °C 3.1: methanesulfonyl chloride; triethylamine / dichloromethane / 2 h / 0 - 20 °C View Scheme
参考文献
Suarez Del Villar, Irene; Gradillas, Ana; Perez-Castells, Javier
European Journal of Organic Chemistry, 2010 , # 30 p. 5850 - 5862
反应条件
1.1: tetrahydrofuran / 0.5 h / 20 °C 1.2: 1 h / 80 °C 2.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -78 °C 3.1: methanesulfonyl chloride; triethylamine / dichloromethane / 2 h / 0 - 20 °C View Scheme
参考文献
Suarez Del Villar, Irene; Gradillas, Ana; Perez-Castells, Javier
European Journal of Organic Chemistry, 2010 , # 30 p. 5850 - 5862
反应条件
1: 0.05 g / H2O; ethanol / 72 h / 27 °C / Beauveria Sulfurescens; pH 4.85 2: Ambient temperature View Scheme
参考文献
Archelas, Alain; Furstoss, Roland; Srairi, Driss; Maury, Georges
Bulletin de la Societe Chimique de France, 1986 , # 2 p. 234 - 238
