2-[(己基氨基)甲基]苯酚合成路线 (共 11 条)
参考文献
Takahashi, Masami; Kuroda, Tooru; Ogiku, Tsuyoshi; Ohmizu, Hiroshi; Kondo, Kazuhiko; Iwasaki, Tameo
Heterocycles, 1992 , vol. 34, # 11 p. 2061 - 2064
反应条件
1: 1) Et3N / 1) DMA, r.t., 6 h, 2) r.t., 14 h
2: 90 percent / Cu / dimethylformamide / 1 h / Heating
3: 70 percent / CH2Cl2 / 96 h / Ambient temperature
View Scheme
参考文献
Takahashi, Masami; Ogiku, Tsuyosi; Okamura, Kimio; Da-te, Tadamasa; Ohmizu, Hiroshi; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 13 p. 1473 - 1480
反应条件
in dichloromethane
96 h; Ambient temperature;
参考文献
Takahashi, Masami; Kuroda, Tooru; Ogiku, Tsuyoshi; Ohmizu, Hiroshi; Kondo, Kazuhiko; Iwasaki, Tameo
Heterocycles, 1993 , vol. 36, # 8 p. 1867 - 1882
反应条件
in dichloromethane
96 h; Ambient temperature;
参考文献
Takahashi, Masami; Kuroda, Tooru; Ogiku, Tsuyoshi; Ohmizu, Hiroshi; Kondo, Kazuhiko; Iwasaki, Tameo
Heterocycles, 1993 , vol. 36, # 8 p. 1867 - 1882
反应条件
1: 89 percent / Cu / dimethylformamide / 1 h / Heating
2: 70 percent / CH2Cl2 / 96 h / Ambient temperature
View Scheme
参考文献
Takahashi, Masami; Ogiku, Tsuyosi; Okamura, Kimio; Da-te, Tadamasa; Ohmizu, Hiroshi; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 13 p. 1473 - 1480
反应条件
in dichloromethane
96 h; Ambient temperature;
参考文献
Takahashi, Masami; Ogiku, Tsuyosi; Okamura, Kimio; Da-te, Tadamasa; Ohmizu, Hiroshi; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 13 p. 1473 - 1480
反应条件
1: 70 percent / KOH / dioxane; H2O / 3 h / Ambient temperature
2: 1) Et3N / 1) DMA, r.t., 6 h, 2) r.t., 14 h
3: 90 percent / Cu / dimethylformamide / 1 h / Heating
4: 70 percent / CH2Cl2 / 96 h / Ambient temperature
View Scheme
参考文献
Takahashi, Masami; Ogiku, Tsuyosi; Okamura, Kimio; Da-te, Tadamasa; Ohmizu, Hiroshi; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 13 p. 1473 - 1480
反应条件
1: 83 percent / cooper / dimethylformamide / Heating
2: methanol
View Scheme
参考文献
Takahashi, Masami; Kuroda, Tooru; Ogiku, Tsuyoshi; Ohmizu, Hiroshi; Kondo, Kazuhiko; Iwasaki, Tameo
Heterocycles, 1992 , vol. 34, # 11 p. 2061 - 2064
反应条件
1: 90 percent / Cu / dimethylformamide / 1 h / Heating
2: 70 percent / CH2Cl2 / 96 h / Ambient temperature
View Scheme
参考文献
Takahashi, Masami; Ogiku, Tsuyosi; Okamura, Kimio; Da-te, Tadamasa; Ohmizu, Hiroshi; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 13 p. 1473 - 1480
反应条件
1: 85 percent / Cu / dimethylformamide / 1 h / Heating
2: 70 percent / CH2Cl2 / 96 h / Ambient temperature
View Scheme
参考文献
Takahashi, Masami; Ogiku, Tsuyosi; Okamura, Kimio; Da-te, Tadamasa; Ohmizu, Hiroshi; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 13 p. 1473 - 1480