2-甲基-5-苯基呋喃-3-羧酸合成路线 (共 17 条)
反应条件
sodium in ethanol 3 h; Heating;
参考文献
Farmaco, Edizione Scientifica, , vol. 42, # 5 p. 629 - 639
反应条件
1: 72 percent / 12 M hydrochloric acid / ethanol / 24 h / Heating 2: 35 percent / pieces of sodium / ethanol / 3 h / Heating View Scheme
参考文献
Farmaco, Edizione Scientifica, , vol. 42, # 5 p. 629 - 639
反应条件
1: 1.) sodium pellets / 1.) toluene, room temp., 3 days, 2.) toluene, 0 deg C, 1 h then room temp., 1 day 2: 72 percent / 12 M hydrochloric acid / ethanol / 24 h / Heating 3: 35 percent / pieces of sodium / ethanol / 3 h / Heating View Scheme
参考文献
Farmaco, Edizione Scientifica, , vol. 42, # 5 p. 629 - 639
反应条件
1: N-bromosuccinmide / N,N-dimethyl-formamide / 0 - 20 °C 2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethylene glycol dimethyl ether; water / 16 h / 85 °C 3: water; lithium hydroxide hydrate / methanol / Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 18 p. 5417 - 5422
反应条件
water; lithium hydroxide hydrate in methanol Reflux;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 18 p. 5417 - 5422
反应条件
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethylene glycol dimethyl ether; water / 16 h / 85 °C 2: water; lithium hydroxide hydrate / methanol / Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 18 p. 5417 - 5422
反应条件
ethanol; dihydrogen peroxide
参考文献
Gazzetta Chimica Italiana, , vol. 87, p. 454,465
反应条件
hydrogenchloride Verseifung des Aethylesters mit alkoh. Kalilauge;
参考文献
Chemische Berichte, , vol. 17, p. 2766
Chemische Berichte, , vol. 18, p. 58
Chemische Berichte, , vol. 17, p. 72
Chemische Berichte, , vol. 18, p. 790
参考文献
Gazzetta Chimica Italiana, , vol. 87, p. 454,465
反应条件
1: acetic acid anhydride 2: aq.-ethanolic KOH-solution View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 87, p. 454,465