1,3,5-三甲基-1H-吡唑-4-甲腈合成路线 （共 8 条）
反应条件
1: in tetrachloromethane T=20°C; 2: With hydrogenchloride in acetone Heating;
参考文献
Calle; Cuadrado; Gonzalez-Nogal; Valero
Synthesis, 2001 , # 13 p. 1949 - 1958
反应条件
in ethanol 3 h; Heating;
参考文献
Alberola; Antolin; Gonzalez; et al.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 4 p. 1035 - 1038
反应条件
acetic anhydride 1 h; Reflux;
参考文献
Attaryan; Sahakyan; Tamazyan; Ayvazyan; Asratyan
Russian Journal of General Chemistry, 2012 , vol. 82, # 10 p. 1720 - 1723
Zh. Obshch. Khim., 2012 , vol. 82, # 10 p. 1716 - 1719,4
反应条件
in ethanol 3 h; Heating;
参考文献
Alberola; Antolin; Gonzalez; et al.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 4 p. 1035 - 1038
反应条件
1.1: BuLi; TMEDA / tetrahydrofuran / 5 h / -78 °C 1.2: 19 percent / tetrahydrofuran / -78 - 0 °C 2.1: CCl4 / 20 °C 2.2: 72 percent / aq. HCl / acetone / Heating View Scheme
参考文献
Calle; Cuadrado; Gonzalez-Nogal; Valero
Synthesis, 2001 , # 13 p. 1949 - 1958
反应条件
1: 81 percent / Heating 2: 70 percent / ethanol / 3 h / Heating View Scheme
参考文献
Alberola; Antolin; Gonzalez; et al.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 4 p. 1035 - 1038
反应条件
in water 3 h; Heating;
参考文献
Alberola; Antolin; Gonzalez; et al.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 4 p. 1035 - 1038
反应条件
1: potassium hydroxide; hydroxylamine hydrochloride / ethanol; water 2: acetic anhydride / 1 h / |Reflux View Scheme
参考文献
Attaryan; Sahakyan; Tamazyan; Ayvazyan; Asratyan
Russian Journal of General Chemistry, 2012 , vol. 82, # 10 p. 1720 - 1723
Zh. Obshch. Khim., 2012 , vol. 82, # 10 p. 1716 - 1719,4
