反应条件
Multi-step reaction with 3 steps 1.1: iPr2NH; BuLi / tetrahydrofuran; hexane / 0.33 h / -78 °C1.2: 70 percent / tetrahydrofuran; hexane / -78 - 0 °C2.1: 70 percent / pyridinium chlorochromate / CH2Cl2 / 2 h / 0 °C3.1: 100 percent Chromat. / NADPH; ketoreductase 102; glucose dehydrogenase / aq. phosphate buffer / 24 h / 37 °C / pH 6.5
参考文献
Kalaitzakis, Dimitris; Rozzell, J. David; Smonou, Ioulia; Kambourakis, Spiros Advanced Synthesis and Catalysis, 2006 , vol. 348, # 14 p. 1958 - 1969