反应条件
Multi-step reaction with 4 steps 1: 1.) magnesium / 1.) diethyl ether, 2.) diethyl ether, reflux, 2 h; 20 deg C, 10 h2: 84 percent / 16 h3: 96 percent / hydrazine / tetrahydrofuran / 12 h / 65 °C4: 65 percent / sodium formate / methanol; H2O / 2 h
参考文献
Baldwin, Jack E.; Adlington, Robert M.; Bottaro, Jeffrey C.; Kolhe, Jayant N.; Newington, Ian M.; Perry, Matthew W. D. Tetrahedron, 1986 , vol. 42, # 15 p. 4235 - 4246
