1: 90 percent / dimethyl sulphoxide - oxalyl chloride, triethylamine / CH2Cl2 / 0.33 h / -55 °C
2: 62 percent / benzene-d6 / 5.58 h / 160 °C
View Scheme
参考文献
Battye, Peter J.; Jones, David W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1479 - 1490
With oxalyl dichloride; dimethyl sulfoxide; triethylamine in dichloromethane T=-55°C; 0.333333 h;
参考文献
Battye, Peter J.; Jones, David W. Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1479 - 1490
