1082725-43-6合成路线 （共 16 条）
反应条件
lithium diisopropyl amide in tetrahydrofuran -75 deg C, 1 h; r.t., 1 h; r.t., 2 h;
参考文献
Tsuge, Otohiko; Sone, Kazuhiro; Urano, Sathoshi
Chemistry Letters, 1980 , p. 977 - 980
反应条件
lithium diisopropyl amide in tetrahydrofuran -75 deg C, 1 h; r.t., 1 h; r.t., 2 h;
参考文献
Tsuge, Otohiko; Sone, Kazuhiro; Urano, Sathoshi
Chemistry Letters, 1980 , p. 977 - 980
反应条件
lithium diisopropyl amide 1.) THF, hexane, -78 deg C, 1 h, 2.) a) from -78 deg C to room temp., 1 h, b) room temp., 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tsuge, Otohiko; Sone, Kazuhiro; Urano, Satoshi; Matsuda, Koyo
Journal of Organic Chemistry, 1982 , vol. 47, # 26 p. 5171 - 5177
反应条件
1: 74 percent / CH2Cl2 / 13 h / Ambient temperature 2: 90 percent / benzene / 30 h / Heating View Scheme
参考文献
Tsuge, Otohiko; Urano, Satoshi; Iwasaki, Takahiko
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 2 p. 485 - 489
反应条件
in N,N-dimethyl-formamide 1) reflux, 1h; 2) overnight, room temp.;
参考文献
Zvezdina, E. A.; Golyanskaya, O. M.; Andreeva, I. M.; Popova, A. N.; Medyantseva, E. A.; Dorofeenko, G. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 4 p. 340 - 343
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 4 p. 457 - 460
反应条件
in dichloromethane 18 h; Ambient temperature;
参考文献
Heterocycles, , vol. 23, # 5 p. 1155 - 1160
反应条件
in chloroform 20 h; Ambient temperature;
参考文献
Journal of Heterocyclic Chemistry, , vol. 28, # 1 p. 89 - 91
反应条件
perchloric acid; water; Annogen in N,N-dimethyl-formamide T=30°C; ΔH(excit.), ΔS(excit.); var. temperature; Rate constantKineticsThermodynamic data;
参考文献
Uma; Gopalakrishnan; Jayabharathi; Thanikachalam
Journal of the Indian Chemical Society, 1996 , vol. 73, # 7 p. 329 - 334
参考文献
Barrow; Griffiths
Journal of the Chemical Society, 1921 , vol. 119, p. 212
反应条件
in ethanol 0.5 h; RefluxGreen chemistry;
参考文献
Kumar, Dhruva; Suresh; Sandhu, Jagir S.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 8 p. 1157 - 1160
