18-crown-6 ether in tetrahydrofuran
T=20°C; 0.25 h; also reaction with α-methylstyrene; MechanismProduct distribution;
参考文献
Jedlinski, Zbigniew; Czech, Aleksander; Janeczek, Henryk; Kowalczuk, Marek
Journal of the American Chemical Society, 1995 , vol. 117, # 33 p. 8678 - 8679
Ren, Peng; Vechorkin, Oleg; Von Allmen, Kim; Scopelliti, Rosario; Hu, Xile
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 7084 - 7095
1: With iron (+/-)-(N,N'-bis(pyridin-2-ylmethylene)cyclohexane-1,2-diamine)dichloride in tetrahydrofuran
T=-20°C; 0.25 h;
2: With LiH3BNMe2 in tetrahydrofuran
T=-20 - 20°C; 16 h;
参考文献
Le Bailly, Bryden A. F.; Greenhalgh, Mark D.; Thomas, Stephen P.
Chemical Communications, 2012 , vol. 48, # 10 p. 1580 - 1582
1: With iron (+/-)-(N,N'-bis(pyridin-2-ylmethylene)cyclohexane-1,2-diamine)dichloride in tetrahydrofuran
T=-20°C; 0.25 h;
2: With LiH3BNMe2 in tetrahydrofuran
T=-20 - 20°C; 16 h;
参考文献
Le Bailly, Bryden A. F.; Greenhalgh, Mark D.; Thomas, Stephen P.
Chemical Communications, 2012 , vol. 48, # 10 p. 1580 - 1582
Ren, Peng; Vechorkin, Oleg; Von Allmen, Kim; Scopelliti, Rosario; Hu, Xile
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 7084 - 7095
Ren, Peng; Vechorkin, Oleg; Von Allmen, Kim; Scopelliti, Rosario; Hu, Xile
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 7084 - 7095
