反应条件
Multi-step reaction with 3 steps 1: triethylamine / dichloromethane / 5 h / 0 - 20 °C2: N,N-dimethyl-formamide; phosgene / dichloromethane / 5 h / 20 °C / |Inert atmosphere3: potassium tri-sec-butyl-borohydride / tetrahydrofuran / 20 °C
参考文献
Bowman, W. Russell; Lyon, Jessica E.; Pritchard, Gareth J. Arkivoc, 2012 , vol. 2012, # 7 p. 210 - 227