alpha-氨基-苯丙酰胺盐酸盐(1:1)合成路线 （共 11 条）
反应条件
ammonia in methanol 96 h; Ambient temperature;
参考文献
Yasukawa, Kazuyuki; Asano, Yasuhisa
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 17 p. 3327 - 3332
反应条件
1: aq. NaOH; Bu4NHSO4 / CH2Cl2 / 20 °C 2: aq. hydrochloric acid View Scheme
参考文献
Hyett, David J.; Didone, Mara; Milcent, Thierry J.A.; Broxterman, Quirinus B.; Kaptein, Bernard
Tetrahedron Letters, 2006 , vol. 47, # 44 p. 7771 - 7774
反应条件
1: thionyl chloride / 0 °C 2: ammonia / methanol / 0 °C View Scheme
参考文献
Yasukawa, Kazuyuki; Asano, Yasuhisa
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 17 p. 3327 - 3332
反应条件
PLP in aq. buffer T=40°C; pH=8.0; 6 h; Enzymatic reaction;
参考文献
Yasukawa, Kazuyuki; Asano, Yasuhisa
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 17 p. 3327 - 3332
反应条件
1: PLP; cobalt(II) chloride / aq. buffer / 4 h / 40 °C / pH 7.0 / |Enzymatic reaction 2: thionyl chloride / 0 °C 3: ammonia / methanol / 0 °C View Scheme
参考文献
Yasukawa, Kazuyuki; Asano, Yasuhisa
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 17 p. 3327 - 3332
反应条件
aminopeptidase from pig's-kidneys; manganese (II) chloride T=38°C; Hydrolysis.pH 7.5;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 31, p. 529,530
反应条件
1: PLP; cobalt(II) chloride / aq. buffer / 4 h / 40 °C / pH 7.0 / |Enzymatic reaction 2: thionyl chloride / 0 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 17 p. 3327 - 3332
反应条件
1: PLP / aq. buffer / 6 h / 40 °C / pH 8.0 / |Enzymatic reaction 2: thionyl chloride / 0 °C 3: ammonia / methanol / 0 °C View Scheme
参考文献
Yasukawa, Kazuyuki; Asano, Yasuhisa
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 17 p. 3327 - 3332
反应条件
1: PLP / aq. buffer / 6 h / 40 °C / pH 8.0 / |Enzymatic reaction 2: thionyl chloride / 0 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 17 p. 3327 - 3332
反应条件
PLP; cobalt(II) chloride in aq. buffer T=40°C; pH=7.0; 4 h; Enzymatic reaction;
参考文献
Yasukawa, Kazuyuki; Asano, Yasuhisa
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 17 p. 3327 - 3332
