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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
108366-84-3
合成路线
（共 6 条）
108366-83-2
→
反应条件
108366-84-3
反应条件
hydrogen in ethanol P=2280 Torr; 4 h; Ambient temperature;
参考文献
Ouchi, Mikio; Inoue, Yoshihisa; Wada, Kazuhito; Iketani, Shin-ichi; Hakushi, Tadao; Weber, Edwin
Journal of Organic Chemistry, 1987 , vol. 52, # 12 p. 2420 - 2427
3663-46-5
(2,2,5-三甲基-[1,3]二噁-5-基)甲醇
→
反应条件
108366-84-3
反应条件
1: 59 percent / Na (methal) / xylene / 2 h / 100 °C 2: 91 percent / H2O, 7 percent HCl 3: 45 percent / NaH / tetrahydrofuran / 12 h / Heating 4: 90 percent / H2 / ethanol / 4 h / 2280 Torr / Ambient temperature View Scheme
参考文献
Ouchi, Mikio; Inoue, Yoshihisa; Wada, Kazuhito; Iketani, Shin-ichi; Hakushi, Tadao; Weber, Edwin
Journal of Organic Chemistry, 1987 , vol. 52, # 12 p. 2420 - 2427
77-85-0
1,1,1-三(羟甲基)乙烷
→
反应条件
108366-84-3
反应条件
1: 96 percent / p-toluenesulfonic acid / 48 h / Ambient temperature 2: 59 percent / Na (methal) / xylene / 2 h / 100 °C 3: 91 percent / H2O, 7 percent HCl 4: 45 percent / NaH / tetrahydrofuran / 12 h / Heating 5: 90 percent / H2 / ethanol / 4 h / 2280 Torr / Ambient temperature View Scheme
参考文献
Ouchi, Mikio; Inoue, Yoshihisa; Wada, Kazuhito; Iketani, Shin-ichi; Hakushi, Tadao; Weber, Edwin
Journal of Organic Chemistry, 1987 , vol. 52, # 12 p. 2420 - 2427
37860-51-8
四乙二醇二对甲苯磺酸酯
→
反应条件
108366-84-3
反应条件
1: 45 percent / NaH / tetrahydrofuran / 12 h / Heating 2: 90 percent / H2 / ethanol / 4 h / 2280 Torr / Ambient temperature View Scheme
参考文献
Ouchi, Mikio; Inoue, Yoshihisa; Wada, Kazuhito; Iketani, Shin-ichi; Hakushi, Tadao; Weber, Edwin
Journal of Organic Chemistry, 1987 , vol. 52, # 12 p. 2420 - 2427
4270-73-9
→
反应条件
108366-84-3
反应条件
1: 45 percent / NaH / tetrahydrofuran / 12 h / Heating 2: 90 percent / H2 / ethanol / 4 h / 2280 Torr / Ambient temperature View Scheme
参考文献
Ouchi, Mikio; Inoue, Yoshihisa; Wada, Kazuhito; Iketani, Shin-ichi; Hakushi, Tadao; Weber, Edwin
Journal of Organic Chemistry, 1987 , vol. 52, # 12 p. 2420 - 2427
87104-70-9
→
反应条件
108366-84-3
反应条件
1: 91 percent / H2O, 7 percent HCl 2: 45 percent / NaH / tetrahydrofuran / 12 h / Heating 3: 90 percent / H2 / ethanol / 4 h / 2280 Torr / Ambient temperature View Scheme
参考文献
Ouchi, Mikio; Inoue, Yoshihisa; Wada, Kazuhito; Iketani, Shin-ichi; Hakushi, Tadao; Weber, Edwin
Journal of Organic Chemistry, 1987 , vol. 52, # 12 p. 2420 - 2427
