N-(5-溴-3-吡啶)苯磺酰胺合成路线 (共 4 条)
反应条件
pyridine T=20°C; 16 h;
参考文献
Cellzome Limited
Patent: WO2009/68482 A1, 2009 ;
Location in patent: Page/Page column 41-42 ;
WO 2009/068482 A1
反应条件
triethylamine in dichloromethane T=0 - 20°C; 1 h;
参考文献
WO2008/150827 A1, ;
Page/Page column 72-73 ;
WO 2008/150827 A1
反应条件
potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=100°C; 18 h;
参考文献
SMITHKLINE BEECHAM CORPORATION
Patent: WO2008/150827 A1, 2008 ;
Location in patent: Page/Page column 73 ;
WO 2008/150827 A1
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in 1,4-dioxane T=100°C; 3 h; Sealed pressure tube;
参考文献
WO2009/39140 A1, ;
Page/Page column 47 ;
WO 2009/039140 A1